corso di analisi dei farmaci lezioni fabrizio melani via sesto fiorentino ( polo scientifico) Dispensa completa – Analisi dei medicinali – a.a. / Porretta: Analisi Quantitativa di composti farmaceutici, (CISU – Roma). nell’ analisi farmaceutica per effettuare la determinazione dei metalli residui nei farmaci. TA – Analisi di Preparazioni Farmaceutiche. E. Abignente, D. Melisi, M.G. Rimoli-Principi di Analisi Quantitativa dei Medicinali- Loghia Napoli. Porretta – Analisi di preparazioni farmaceutiche. CISU. Farmacopea Ufficiale Italiana X Ed. V. Cavrini, V. Andrisano – Principi di ANALISI FARMACEUTICA.

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One apply, to the execution of these determinations, analytical methods by theoretical principles – with the chemistry and the stoichiometry – and the practical applications. Volumetric and strumental methods are employed.

Give the basic knowledge for analyzing and statistically elaborate the data. To take prepparazioni final examination learning assessment proceduresstudents must have passed the exam of General and inorganic chemistry.

Study-unit DRUG ANALYSIS II – Degree Course: Pharmacy

Calculation in volumetric analysis. Direct titration of strong acids and bases. Direct titration of weak acids and bases. Direct titration of polyprotic acid. Direct titration of neutral salt of polyprotic acid. Direct titration of salt of weak acid and base. Back titrations and blank determinations.


Titration of organic acids, organic bases, and halogen salts of organic bases.

Analisi di preparazioni farmaceutiche : analisi quantitativa

Determinations involving the use of potassium permanganate solution. Direct and indirect titrations with iodine. Direct and back-titration with disodium edetate. Definitions of samples, analyte, matrics, determination and analysis.

Requirement of an analytical method. Criteria for selecting a poretta of analysis. Steps in a typical quantitative analysis. Classification of quantitative methods of analysis: Mass and concentration units of measurements. Treatment of experimental data: Evaluation and data presentation. Errors in chemical analyses: Accuracy, precision and outlier. Standard deviation, relative standard deviation, coefficient of variation, confidence interval, absolute and relative error.

Statistical tests for accuracy, precision and outlier evaluation: Comparison of analytical methods in terms of accuracy, precision, sensitivity, specificity. Chemical equilibria in solution: Effects of electrolites on chemical equilibria. Titrimetric methods of analysis: Criteria for the selection and use of chemical acid-base and redox indicators.

Analisi di preparazioni farmaceutiche : analisi quantitativa (Book, ) []

Electrochemical cells, electrode potentials; Nernst equation. Reference electrodes, indicators electrodes. Direct potentiometric measurements ion sensitive electrodes and indirect measurements potentiometric titrations. Instrumental calibration and applications. During the lectures, general principles of analytic methods and instructions for the practical work are explained through oral exposition with blackboard support.

The practical exercises are in the afternoonin a span of 4h a day.


The instrumental methods are applied with a support of a technician. Oral presentation supported by blackboard, analis an powerpoint. General principles 7 h Purposes of the titration reactions. Titration curves 3 h Potenziometric analysis. Reference and indicator electrodes. Principles for a quantitative analysis in the UV range 4 h Chromatography: Chromatographic parameters 6 h Introduction to data analysis. Errors, accuracy and precision.

Error propagation in the calculations 3 h Stoichiometric exercises Learning assessment procedures The examination consists in a written and oral tests, aimed to assess and measure a test-taker’s knowledge, skill, and aptitude towards the whole content of the two teaching units. The written part consists in three stoichiometry exercices Analytical Chemistry unit and two questions regarding the practical part Quantitative analysis of drug.

The final score accounts of the partial evaluation of the written and oral tests and of the quality of the practical part. Analisi quantitativa del farmaco e chimica analitica. Modulo di Chimica analitica Prof. Modulo di Analisi quantitativa del farmaco Prof. Dipartimento di Scienze della Vita e Biotecnologie Coordinatore: Via Luigi Borsari 46 – Ferrara Guarda la mappa.